Chemistry Experiments for Instrumental Methods
, by Sawyer, Donald T.; Heineman, William R.; Beebe, Janice M.
- ISBN: 9780471893035 | 047189303X
- Cover: Paperback
- Copyright: 1/16/1991
The only self-contained modern laboratory manual for advanced undergraduate courses in instrumental analysis. Consists of over 50 experiments demonstrating the theory and practice of electrochemical methods, methods based on electromagnetic radiation, and separation methods. Experiments are introduced with a review of the physical principles on which the experimental procedures are based.
DONALD T. SAWYER is Distinguished Professor of Chemistry at Texas A&M University, and from 1956 to 1986 was on the faculty of the University of California, Riverside. Professor Sawyer is the author of 300 research publications and coauthor of ten books, including Experimental Electrochemistry for Chemists, and Electrochemical Studies of Biological Systems. His numerous awards and appointments include election as a Fellow of the American Association for the Advancement of Science; Guggenheim, Merton College, and JSPS Fellowships; and the Richard C. Tolman Medal.
| Preface | xiii | ||||
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1 | (6) | |||
| Part 1 Electrochemical Methods | 7 | (154) | |||
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9 | (49) | |||
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24 | (4) | |||
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28 | (5) | |||
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31 | (1) | |||
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58 | (14) | |||
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63 | (6) | |||
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126 | (6) | |||
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144 | (17) | |||
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148 | (2) | |||
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150 | (1) | |||
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151 | (4) | |||
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155 | (6) | |||
| Part 2 Methods Based on Electromagnetic Radiation | 161 | (158) | |||
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163 | (52) | |||
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168 | (13) | |||
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180 | (1) | |||
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242 | (24) | |||
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254 | (4) | |||
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266 | (20) | |||
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270 | (6) | |||
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276 | (3) | |||
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279 | (4) | |||
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284 | (2) | |||
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286 | (33) | |||
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293 | (2) | |||
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297 | (4) | |||
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301 | (1) | |||
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304 | (4) | |||
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308 | (1) | |||
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309 | (3) | |||
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312 | (5) | |||
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317 | (2) | |||
| Part 3 Separation Methods | 319 | (84) | |||
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321 | (23) | |||
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328 | (5) | |||
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333 | (3) | |||
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336 | (2) | |||
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338 | (3) | |||
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341 | (3) | |||
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344 | (17) | |||
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361 | (6) | |||
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364 | (3) | |||
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367 | (13) | |||
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369 | (5) | |||
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374 | (6) | |||
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380 | (7) | |||
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382 | (2) | |||
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384 | (3) | |||
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387 | (9) | |||
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390 | (6) | |||
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396 | (7) | |||
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400 | (3) | |||
| Appendices | 403 | ||||
| Appendix 1 / Special Project Experiments from the Journal of Chemical Education, 1972-1982 | 405 | (5) | |||
| Appendix 2 / Reference Tables | 410 | ||||
| Table A-1 Physical Constants and Units | 410 | (1) | |||
| Table A-2 SI Derived Units | 411 | (1) | |||
| Table A-3 Acidity Constants of Inorganic Substances | 412 | (1) | |||
| Table A-4 Acidity Constants of Organic Substances | 413 | (1) | |||
| Table A-5 Acid-Base Indicators | 414 | (1) | |||
| Table A-6 Solubility-Product Constants | 415 | (1) | |||
| Table A-7 Formation Constants (log K) of Some Metal Chelonates | 416 | (3) | |||
| Table A-8 Formation Constants of Some Metal Complexes | 419 | (1) | |||
| Table A-9 Standard and Formal Electrode Potentials at 25 degree C | 420 | (4) | |||
| Table A-10 Potentials of the Common Reference Electrodes | 424 | (1) | |||
| Table A-11 Equivalent Ionic Conductances at Infinite Dilution | 424 | (1) | |||
| Table A-12 Polarographic Half-Wave Potentials | 425 | (1) | |||
| Table A-13 Spectrophotometric Solvents for UV and IR Spectra | 426 | (1) | |||
| Table A-14 Useful Spectral Regions for Absorption Cells and Instruments | 426 | (1) | |||
| Table A-15 Emission Spectra; Principal Analysis Lines of the Elements | 427 |
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