Ion Exchange and Solvent Extraction: A Series of Advances, Volume 15

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ISBN: 9780824706012 | 0824706013
Cover: Hardcover
Copyright: 10/12/2001

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"Contains a complete manual with procedures for the implementation and scaling-up of industrial extraction processes. Discusses computer-aided molecular design. Includes examples of interactive, combinatorial, construct-and-test, and mathematical programming. "

Preface

iii

Contributors to Volume 15

vii

Contents of Other Volumes

xiii

An Integrated Method for Development and Scaling Up of Extraction Processes

(106)

Baruch Grinbaum

Introduction

(2)

Project Definition and Analysis

(13)

Laboratory Development of an SX Process

(5)

Process Simulation

(12)

Physical, Hydrodynamic, and Kinetic Data

(13)

Summary of the Laboratory Stage

(12)

Piloting

(42)

Process Book (Recommendations and Scaling Up)

100

(7)

References

105

(2)

Design of Pulsed Extraction Columns

107

(36)

Alfons Vogelpohl

Hartmut Haverland

Introduction and Design Concept

107

(1)

Population Balance Model

108

(1)

Experimental Studies

109

(15)

Simulation of Pulsed Extraction Columns

124

(6)

Comparison of Experimental and Simulated Results

130

(6)

Summary and Outlook

136

(7)

Notation

139

(2)

References

141

(2)

Purification of Nickel by Solvent Extraction

143

(54)

Kathryn C. Sole

Peter M. Cole

Introduction

143

(1)

Mineralogy of Nickel Ores and Its Implications for the Choice of Process Routes

144

(2)

Chemistry of Nickel Separations by Solvent Extraction

146

(8)

Early Commercial Processes Using Solvent Extraction in the Purification of Nickel

154

(3)

Second-Generation Processes

157

(6)

Modern Flow Sheets for the Hydrometallurgical Processing of Nickel

163

(12)

Current Developments and Pilot Plant Trials

175

(14)

Conclusions

189

(8)

References

190

(7)

Treatment of Soils and Sludges by Solvent Extraction in the United States

197

(24)

Richard J. Ayen

James D. Navratil

Technology Concepts

197

(6)

Developed Solvent Extraction Technologies

203

(10)

Summary of Commercial Applications

213

(8)

References

216

(5)

The Design of Solvents for Liquid-Liquid Extraction

221

(34)

Braam van Dyk

Izak Nieuwoudt

Introduction

221

(1)

Solvent Selection Methods

222

(5)

Designer Solvents: The State of the Art

227

(11)

Designer Solvents: An Evolutionary Approach

238

(11)

A Case Study in Evolutionary Solvent Design

249

(2)

Conclusions

251

(4)

References

252

(3)

Extraction Technology for the Separation of Optical Isomers

255

(40)

Andre B. de Haan

Bela Simandi

Introduction

255

(1)

Current Chiral Manufacturing and Separation Technology

256

(2)

Principles of Enantioselective Extraction

258

(6)

Liquid-Liquid Extraction

264

(9)

Liquid Membranes

273

(4)

Supercritical Fluid Extraction

277

(4)

Aqueous Two-Phase Extraction

281

(3)

Membrane Filtration Assisted Extraction

284

(2)

Future Outlook

286

(9)

References

290

(5)

Regularities of Extraction in Systems on the Basis of Polar Organic Solvents and Use of Such Systems for Separation of Important Hydrophobic Substances

295

(36)

Sergey M. Leschev

Introduction

295

(1)

Methodology

296

(3)

Phenomenological Description of the Extraction Process

299

(2)

Group Increments and Their Use for the Description and Prediction of the Extraction of Various Substances

301

(7)

Mutual Solubility of Phase Components and Its Influence on Group Increments

308

(3)

Determination of Gibbs Energies of Solvation of Organic Nonelectrolytes Based on Their Distribution

311

(3)

The Solvophobic Effect of the Polar Phase and Its Influence on Extraction

314

(5)

Extraction, Separation, Isolation, and Preconcentration of Natural and Synthetic Hydrophobic Organic Substances

319

(9)

Concluding Remarks

328

(3)

References

328

(3)

Developments in Dispersion-Free Membrane-Based Extraction-Separation Processes

331

(140)

Anil Kumar Pabby

Ana-Maria Sastre

Introduction

331

(4)

Developments in Dispersion-Free Membrane Extraction

335

(1)

Membrane-Based Liquid---Liquid Extraction (MLLE)

335

(56)

Emulsion and Bulk Liquid Membranes Utilizing Hollow-Fiber Contactors

391

(10)

Modeling of Hollow-Fiber, Membrane-Based, Liquid---Liquid Extraction (HFMLLE) and Kinetic Analysis

401

(47)

Special Uses of Hollow-Fiber Membranes and Contactors

448

(6)

Concluding Remarks and Future Trends

454

(3)

Trade Names, Abbreviations, and Symbols

457

(14)

References

463

(8)

Index

471

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Ion Exchange and Solvent Extraction: A Series of Advances, Volume 15

Summary

Table of Contents

Supplemental Materials