Laboratory Experiments to Accompany General, Organic and Biological Chemistry An Integrated Approach

Charles Anderson and David B. Macaulay are the authors of Laboratory Experiments to Accompany General, Organic and Biological Chemistry: An Integrated Approach, 3rd Edition, published by Wiley.

A Note From the Publisher . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v

Safety in the Laboratory. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Suggested Equipment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Fundamental Laboratory Operations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Experiment 1 Measurement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Experiment 2 Some Laboratory Techniques. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Experiment 3 Ions: Role in Nutrition . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Experiment 4 Paper and Thin Layer Chromatography. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69

Experiment 5 Molecules: Organic Compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Experiment 6 Properties of Water . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107

Experiment 7 Chemical Reactions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123

Experiment 8 Stoichiometry: Mole Relationships . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139

Experiment 9 Properties of Gases. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 151

Experiment 10 Acids, Bases, Buffers, and Antacids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 169

Experiment 11 Organic Oxygen Compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189

Experiment 12 Aspirin and Related Compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 207

Experiment 13 Organic Nitrogen Compounds . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 221

Experiment 14 Carbohydrates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 233

Experiment 15 Lipids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 253

Experiment 16 Proteins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267

Experiment 17 Enzymes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 281

Experiment 18 Urine . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 293

Experiment 19 Nucleosides. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305

Experiment 20 DNA and RNA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315

Appendix A Exercise on Chemical Periodicity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 327

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