Microscale and Miniscale Organic Chemistry

This book offers a comprehensive introductory treatment of the organic laboratory techniques for handling glassware and equipment, safety in the laboratory, micro- and miniscale experimental procedures, theory of reactions and techniques, relevant background information, applications and spectroscopy.

1 Techniques in the Organic Laboratory

2 Spectroscopic Methods

3 Introduction to Organic Compounds, Solvents, Separations and Recrystallizations

4 Alcohols and Alkyl Halides

5 Synthesis of Alkenes

6 Alkene Addition Reactions

7 Molecular Modeling and Stereochemistry

8 Introduction to Nucleophilic Substitution Reactions

9 Dienes and Conjugation

10 Qualitative Organic Analysis I

11 Reactions of Aromatic Sidechains

12 Electrophilic Aromatic Substitution

13 Combined Spectroscopy and Advanced Spectroscopy

14 Organometallics

15 Alcohols and Diols

16 Ethers

17 Aldehydes and Ketones

18 Enols and Enolates

19 Carboxylic Acids

20 Carboxylic Acid Derivatives

21 Multistep Preparations

22 Amines

23 Aryl Halides

24 Phenols

25 Carbohydrates

26 Lipids

27 Amino Acids and Proteins

28 Qualitative Organic Analysis II

29 Special Investigations

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Microscale and Miniscale Organic Chemistry Laboratory Experiments

Summary

Table of Contents

Supplemental Materials