Analytical Solid-Phase Extraction

SOLID-PHASE MICROEXTRACTION Theory and Practice Janusz Pawliszyn 1997 (0-471-19034-9) 264 pp.

JAMES S. FRITZ is Distinguished Professor in the Department of Chemistry at Iowa State University. Widely published in solid-phase extraction, he is a recipient of the ACS Award in Chromatography and the ACS Award in Analytical Chemistry.

Preface

xi

Acknowledgments

xiii

Introduction And Principles

1

(14)

Introduction

1

(3)

Principles

4

(9)

Advantages of SPE

13

(2)

SPE In The 1970s: Extraction Of Organic Pollutants From Water

15

(13)

Introduction

15

(2)

Comparison Between Activated Carbon and Porous Resin Adsorbents

17

(1)

Purification of Resins

17

(1)

Sampling and Sample Handling

18

(3)

Preparation of Standards

21

(1)

General Procedure for SPE

22

(4)

Recovery Data

26

(2)

Solid Particles For Solid-Phase Extraction Of Organic Compounds From Water

28

(35)

Introduction

28

(1)

Desirable Properties of SPE Particles

29

(5)

Bonded-Phase Silica Particles

34

(5)

Organic Polymeric Adsorbents

39

(12)

Carbons

51

(3)

Comparison of Sorbents

54

(2)

Molecular Sieves

56

(2)

Sorbents for Normal-Phase SPE

58

(2)

Other Sorbents

60

(3)

Practical Considerations: Equipment And Techniques

63

(26)

The Four Steps of Solid-Phase Extraction

63

(4)

Apparatus

67

(4)

Completeness of Extraction

71

(6)

Elution

77

(4)

Solid Samples and Slurries

81

(2)

Automation

83

(6)

ION-Exchange Sorbents

89

(29)

Introduction

89

(3)

Ion-Exchange SPE Processes

92

(4)

Retention of Neutral Analytes by Sulfonated Resins

96

(5)

Retention of Cations by Sulfonated Resins; Group Separations

101

(8)

SPE with Anion-Exchange Resins

109

(9)

Resin-Loaded Membranes

118

(22)

Introduction

118

(3)

Types of SPE Disks

121

(1)

Techniques for Membrane SPE

122

(3)

Semimicrodisk Extraction

125

(1)

Recovery of Test Compounds Using Membrane Disks

126

(4)

Applications

130

(7)

Conclusions

137

(3)

Preconcentration Of Metal Ions

140

(21)

Introduction

140

(1)

Ion-Exchange Methods

141

(3)

Extraction of Ion-Association Complexes

144

(3)

Extraction of Metal-Organic Complexes

147

(7)

Chelating Resins

154

(3)

Some Conclusions

157

(4)

Microscale And Semimicroscale Techniques

161

(24)

Solid-Phase Microextraction (SPME)

161

(11)

Semimicro Solid-Phase Extraction (SM-SPE)

172

(7)

Miniaturized Solid-Phase Extraction (M-SPE)

179

(4)

Conclusions

183

(2)

Applications

185

(18)

Introduction

185

(1)

Sample Types

186

(8)

Techniques

194

(3)

Problems with Practical Samples

197

(2)

Applications According to Chemical Class

199

(4)

Index

203

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Analytical Solid-Phase Extraction

Summary

Author Biography

Table of Contents

Supplemental Materials

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Analytical Solid-Phase Extraction

Summary

Author Biography

Table of Contents

Supplemental Materials

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