Basic Gas Chromatography

, by McNair, Harold M.; Miller, James M.

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ISBN: 9780470439548 | 0470439548
Cover: Hardcover
Copyright: 7/7/2009

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This is the second, updated edition of the very successful first edition by these co-authors. It contains up-to-date information on the field and has been expanded by several chapters, including one on multidimensional gas chromatography and another on sampling methods, as well as special injection techniques and fast gas chromatography. The new edition offers a brief introduction to GC that should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject.

Preface to the Second Edition	p. ix
Preface	p. xi
Acknowledgments	p. xiii
Introduction	p. 1
A Brief History	p. 1
Definitions	p. 3
Overview: Advantages and Disadvantages	p. 9
Instrumentation	p. 11
References	p. 13
Instrument Overview	p. 14
Carrier Gas	p. 15
Flow Control and Measurement	p. 16
Sample Inlets and Sampling Devices	p. 20
Columns	p. 23
Temperature Zones	p. 24
Detectors	p. 27
Data Systems	p. 27
References	p. 28
Basic Concepts and Terms	p. 29
Definitions, Terms, and Symbols	p. 29
The Rate Theory	p. 40
A Redefinition of H	p. 50
The Achievement of Separation	p. 51
References	p. 52
Stationary Phases	p. 53
Selecting a Column	p. 53
Classification of Stationary Phases for GLC	p. 54
Liquid Stationary Phases (GLC)	p. 65
Solid Stationary Phases (GSC)	p. 69
References	p. 69
Packed Columns and Inlets	p. 71
Solid Supports	p. 71
Liquid Stationary Phases	p. 73
Solid Stationary Phases (GSC)	p. 74
Gas Analysis	p. 76
Analysis of Other Inorganics	p. 80
Inlets for Liquid Samples and Solutions	p. 80
Special Columns	p. 81
Upgrading for Capillary Columns	p. 82
References	p. 83
Capillary Columns and Inlets	p. 84
Types of OT Columns	p. 84
OT Column Tubing	p. 86
Advantages of OT Columns	p. 89
Column Selection	p. 91
Capillary Inlet Systems	p. 97
Miscellaneous Topics	p. 100
References	p. 102
Detectors	p. 104
Classification of Detectors	p. 105
Detector Characteristics	p. 108
Flame Ionization Detector (FID)	p. 115
Thermal Conductivity Detector (TCD)	p. 119
Electron Capture Detector (ECD)	p. 122
Other Detectors	p. 125
References	p. 127
Qualitative and Quantitative Analysis	p. 129
Qualitative Analysis	p. 129
Quantitative Analysis	p. 135
References	p. 144
Programmed Temperature	p. 145
Temperature Effects	p. 145
Advantages and Disadvantages of PTGC	p. 147
Requirements of PTGC	p. 149
Theory of PTGC	p. 151
Special Topics	p. 153
References	p. 155
Gas Chromatography-Mass Spectrometry (GC-MS)	p. 156
Instrumentation	p. 157
History	p. 165
Limitations of GC-MS Systems	p. 166
Data Analysis	p. 167
References	p. 169
Multidimensional Gas Chromatography	p. 170
Overview	p. 170
Fundamental Principles of Multidimensional Chromatography	p. 171
GC×GC with Heart Cutting	p. 174
Comprehensive GC×GC	p. 175
LC×GC with Heart Cutting	p. 178
Comprehensive LC×GC	p. 179
Summary	p. 180
References	p. 181
Sampling Methods	p. 183
Overview	p. 183
Liquid-Liquid Extraction (LLE)	p. 185
Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE)	p. 188
Liquid-Solid Extraction: Solid-Phase Extraction (SPE)	p. 189
Liquid- or Solid-Vapor Extraction: Headspace Extraction	p. 191
Solid-Phase Micro-extraction (SPME)	p. 193
Additional Techniques and Summary	p. 195
References	p. 197
Special Topics	p. 198
Fast GC	p. 198
Chiral Analysis by GC	p. 201
GC Analysis of Nonvolatile Compounds	p. 202
References	p. 205
Troubleshooting GC Systems	p. 207
Symbols and Acronyms	p. 215
Guidelines for Selecting Capillary Columns	p. 218
GC: How to Avoid Problems	p. 220
Calculation of Split Ratio for Split Injection on OT Columns	p. 222
Operating Conditions for Capillary Columns	p. 224
OV Liquid Phases Physical Property Data	p. 225
Some Compressibility Correction Factors (J)	p. 227
Some Internet Websites for Gas Chromatographers	p. 228
Other Books on Gas Chromatography	p. 230
Index of Applications	p. 231
Index	p. 233
Table of Contents provided by Ingram. All Rights Reserved.

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Basic Gas Chromatography

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