A Century of Separation Science

A Century of Separation Science presents an historical, as well as technical, perspective of the critical developments in separation science since 1900, covering recent advances in chromatography, electrophoresis, field-flow fractionation, countercurrent chromatography, and supercritical fluid chromatography for high-speed and high-throughput analysis. The author also discusses the theory of gradient elution and solvent selection for optimal separation in liquid chromatography.

Preface

v

Contributors

xi

Chromatography: The Separation Technique of the Twentieth Century

1

(18)

Leslie S. Ettre

Mikhail Semenovich Tswett: The Father of Modern Chromatography

19

(8)

Haleem J. Issaq

Victor G. Berezkin

From Crushed Bricks to Microchips

27

(22)

Johan Roeraade

Thin Layer Chromatography

49

(20)

Joseph Sherma

From Thin Layer Chromatography to High-Performance Thin Layer Chromatography to Planar Chromatography

69

(18)

Antoine-Michel Siouffi

The Way It Was

87

(14)

Raywond P. W. Scott

Gas Chromatography: A Personal Retrospective

101

(14)

John V. Hinshaw

The Evolution of Capillary Column Gas Chromatography: A Historical Overview

115

(30)

Leslie S. Ettre

Forty Years in Gas Chromatography

145

(12)

Victor G. Berezkin

Liquid Crystal Stationary Phases in Gas Chromatography: A Historic Perspective

157

(22)

George M. Janini

Quantitative Retention-Eluent Composition Relationships in Partition and Adsorption Chromatography

179

(18)

Edward Soczewinski

Hollow Sticks with Mud Inside: The Technology of HPLC Columns

197

(14)

Uwe Dieter Neue

On the Way to a General Theory of Gradient Elution

211

(20)

Pavel Jandera

Solvent Selection for Optimal Separation in Liquid Chromatography

231

(22)

Haleem J. Issaq

My Life in Separation Sciences: Study of Separation Mechanisms

253

(12)

Kiyokatsu Jinno

Travels of a Chromatographer

265

(12)

Fred E. Regnier

The Role of High-Performance Liquid Chromatography and Capillary Electrophoresis in Life Sciences

277

(6)

Phyllis R. Brown

Half a Century in Separation Science

283

(10)

Hamish Small

Development of Countercurrent Chromatography and Other Centrifugal Separation Methods

293

(16)

Yoichiro Ito

Gel Permeation Chromatography/Size Exclusion Chromatography

309

(18)

Jack Cazes

From Metal Organic Chemistry to Chromatography and Stereochemistry

327

(22)

Volker Schurig

Developments in Surface Chemistry for the Improvement of Chromatographic Methods

349

(16)

Joseph J. Pesek

Maria T. Matyska

Multimodal Chromatography and Gel Electrophoresis

365

(8)

Haleem J. Issaq

Field Flow Fractionation

373

(6)

Haleem J. Issaq

The Impact of Analytical Supercritical Fluid Extraction and Supercritical Fluid Chromatography on Separation Science

379

(20)

Jerry W. King

Solid Phase Microextraction

399

(22)

Janusz Pawliszyn

Uppsala School in Separation Science: My Contributions and Some Personal Reflections and Comments

421

(32)

Stellan Hjerten

A Decade of Capillary Electrophoresis

453

(30)

Haleem J. Issaq

Electrophoretic Separation-Based Sensors

483

(22)

Julie A. Lapos

Andrew G. Ewing

High Temperature and Temperature Programming in Pressure-Driven and Electrically Driven Chromatography

505

(16)

Nebojsa M. Djordjevic

Gradient Elution in Capillary Electrophoresis, Micellar Electrokinetic Chromatography, Capillary Electrochromatography, and Microfluidics

521

(6)

Haleem J. Issaq

A History of the Use and Measurement of Affinity Interactions in Electrophoresis

527

(28)

Niels H. H. Heegaard

Direct Enantiomeric Separations in Liquid Chromatography and Gas Chromatography

555

(24)

Daniel W. Armstrong

Chiral Capillary Electrophoresis

579

(10)

Salvatore Fanali

Whole Column Imaging Detection for Capillary Isoelectric Focusing

589

(12)

Xin-Zheng Wu

Jiaqi Wu

Janusz Pawliszyn

Separation Science in Routine Clinical Analysis

601

(10)

Zak K. Shihabi

Moving Microminiaturized Electrophoresis into the Clinical Laboratory

611

(8)

James P. Landers

A Quarter Century of Separation Science, from Paper Chromatography to Capillary Electrophoresis

619

(12)

Haleem J. Issaq

A Personal Perspective on Separation Science

631

(12)

Edward S. Yeung

The 1999 Belgian Dioxin Crisis: The Need to Apply State-of-the-Art Analytical Methods

643

(10)

Pat Sandra

Frank David

Research on Separation Methods at the Max Planck Institut Between 1957 and 1995

653

(14)

Gerhard Schomburg

The Secret Memories of a Member of the Blue Finger Society: A Quarter Century in Polymer Chemistry

667

(18)

Pier Giorgio Righetti

Fishing for Molecules in Biological Soup: From Liquid Chromatography/Electrochemistry to Liquid Chromatography/Mass Spectrometry

685

(8)

Peter T. Kissinger

Adventures in Analytical Chemistry/Biochemistry/Biotechnology

693

(16)

Ira S. Krull

A Czech's Life in Separation Science

709

(12)

Zdenek Deyl

Stagnation and Regression Concomitant with the Advances in Electrophoretic Separation Science

721

(8)

Andreas Chrambach

Lab-on-a-Chip: A Twentieth-Century Dream, a Twenty-First-Century Reality

729

(12)

Daniel Figeys

Jian Chen

Appendix: Selected Readings

741

(10)

Index

751

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A Century of Separation Science

Summary

Table of Contents

Supplemental Materials