Characterization of Porous Solids VI

, by Rodríguez-Reinoso; McEnaney; Rouquerol; Unger

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ISBN: 9780444512611 | 0444512616
Cover: Hardcover
Copyright: 11/14/2002

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This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002. Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

Preface

Committees

xvii

Financial support

xvii

Scanning probe microscopies for the characterization of porous solids: strengths and limitations

(10)

J.I. Paredes

A. Martinez-Alonso

J.M.D. Tascon

Role of gas adsorption in nanopore characterization

(8)

K. Kaneko

T. Ohba

Y. Hattori

M. Sunaga

H. Tanaka

H. Kanoh

Reconstruction method for the characterization of porous carbons

(8)

J. Pikunic

C. Clinard

N. Cohaut

K.E. Gubbins

J.-M. Guet

R.J.-M. Pellenq

I. Rannou

J.-N. Rouzaud

A new method for microporosity detection based on the use of the corrugated pore structure model (CPSM)

(8)

C.E. Salmas

V.N. Stathopoulos

A.K. Ladavos

P-J. Pomonis

G.P. Androutsopoulos

Physisorption in nanopores of various sizes and shapes: a Grand Canonical Monte Carlo simulation study

(8)

B. Coasne

A. Grosman

C. Ortega

R.J.M. Pellenq

Induced porosity in cross-linked polymer networks: Mean field theory and simulations

(8)

S. Srebnik

Microbean small angle X-ray scattering (μSAXS): a novel technique for the characterization of activated carbon fibers

(8)

D. Lozano-Castello

E. Raymundo-Pinero

D. Cazorla-Amoros

A. Linares-Solano

M. Muller

C. Riekel

``Real time'' determination of porosity development in carbons: a combined SAXS/TGA approach

(8)

J.M. Calo

P.J. Hall

S. Houtmann

D. Lozano-Castello

R.E. Winans

S. Seifert

SANS investigations of adsorption mechanisms in model porous silicas

(8)

S. Kallus

A. Hahn

J.D.F. Ramsay

Preparation and surface characterization of novel ceria-copper and ceria-manganese mixed oxides

(8)

M. Christophidou

C.R. Theocharis

About the exclusive mesoporous character of MCM-41

(8)

A. Berenguer-Murcia

J. Garcia-Martinez

D. Cazorla-Amoros

A. Martinez-Alonso

J.M.D. Tascon

A. Linares-Solano

Incorporation of appropriate contact angles in textural characterization by mercury porosimetry

(8)

J.C. Groen

L.A.A. Peffer

J. Perez-Ramirez

A two-stage Horvath-Kawazoe adsorption model for pore size distribution analysis

(8)

R.J. Dombrowski

C.M. Lastoskie

Textural and chemical characterization of NaX zeolite exchanged with Zn(II) ions

107

(8)

J. Silvestre-Albero

A. Sepulveda-Escribano

F. Rodriguez-Reinoso

Evaluation and comparison of the pore structure and related properties of particulate and monolithic silicas for liquid phase separation processes

115

(8)

K.K. Unger

B. Bilingmaier

C. du Fresne von Hohenesche

D. Lubda

Percolation phenomena in micropores: influence on single and multicomponent adsorption equilibria

123

(8)

S. Ismadji

S.K. Bhatia

Characterization of the surface chemistry of activated carbon by molecular simulation of water adsorption

131

(8)

M. Jorge

N.A. Seaton

Comparison of porous carbons developed via templating approaches

139

(8)

P.M. Barata-Rodrigues

T.J. Mays

N.A. Seaton

G.D. Moggridge

Simulation of adsorption in 3-D reconstructed mesoporous materials by a simulated annealing algorithm

147

(8)

M.E. Kainourgiakis

E.S. Kikkinides

G.Ch. Charalambopoulou

A.K. Stubos

Understanding adsorption hysteresis in porous glasses and other mesoporous materials

155

(8)

H.-J. Woo

L. Sarkisov

P.A. Monson

Structural studies of mesoporous alumina membranes by small angle X-ray scattering

163

(8)

J.C. Dore

D. Grandjean

R.E. Benfield

M. Kroll

D. Le Bolloc'h

Assessing microporosity by immersion microcalorimetry into liquid nitrogen or liquid argon

171

(6)

J. Rouquerol

P. Llewellyn

R. Navarrete

F. Rouquerol

R. Denoyel

The lower closure point of the adsorption hysteresis loop of fluids in mesoporous silica materials

177

(8)

A. Schreiber

S. Reinhardt

G.H. Findenegg

New metodologies in mercury porosimetry

185

(8)

S.P. Rigby

Theoretical calculation of high micropore volumes on activated carbons

193

(8)

J. Alcaniz-Monge

Assessment of ultramicroporosity on carbon molecular sieves by water adsorption

201

(8)

J. Alcaniz-Monge

D. Lozano-Castello

Active surface area of carbon materials determined by different methods

209

(8)

A. Arenillas

F. Rubiera

J.B. Parra

J.J. Pis

Heterogeneity of sewage sludge derived materials as a factor governing their performance as adsorbents of acidic gases

217

(8)

A. Bagreev

S. Bashkova

B. Reznik

V. Zibat

T.J. Bandosz

Evaluation of microporous structure of carbon molecular sieves using the pycnometric method

225

(6)

M. Balys

B. Buczek

E. Vogt

Characterization of porous carbonaceous sorbents using adsorption data in wide temperature and pressure ranges

231

(8)

G. De Weireld

M. Frere

Ammonia accessibility to the porosity of several activated carbons measured by flow adsorption microcalorimetry

239

(8)

M. Domingo-Garcia

A.J. Groszek

F.J. Lopez-Garzon

M. Perez-Mendoza

An IGC and TA study of acetaldehyde adsorption on activated carbons

247

(8)

Y. El-Sayed

T.J. Bandosz

A novel approach for characterizing carbon catalysts by TAP experiments

255

(6)

V. Fierro

M.T. Izquierdo

Y. Schuurman

B. Rubio

C. Mirodatos

Preparation of activated carbons with controlled pore size

261

(6)

M.M.A. Freitas

J.L. Figueiredo

Characterization of porous solids using low pressure VOC adsorption data

267

(8)

J. Nokerman

S. Dutour

M. Frere

S. Limborg-Noetinger

S. Jullian

Energetics and mechanism of physical sorption by carbonaceous solids: Evaluation of surface area and porosity factors

275

(8)

E.L. Fuller, Jr.

Phenanthrene adsorption on a carbonaceous material: moisture and CO2 influence

283

(8)

A.M. Mastral

T. Garcia

R. Murillo

M.S. Callen

J.M. Lopez

M.V. Navarro

Water adsorption on micro and mesoporous silicas

291

(8)

J. Alcaniz-Monge

D. Lozano-Castello

The effect of surface functionalization of mesoporous silicas with propylimidazol on porosity, pore connectivity and tortuosity

299

(8)

G.S. Armatas

C.E. Salmas

G.P. Androutsopoulos

P.J. Pomonis

Preparation of porous silica by acid activation of metakaolins

307

(8)

C. Belver

M.A. Banares

M.A. Vicente

The effect of particle shape on the filtration rate and shear strength of quartz and dolomite mineral filter cakes

315

(8)

B. Benli Gonul

O. Ozcan

Characterisation of silica low-density xerogels in presence of additives by image analysis and nitrogen adsorption-desorption

323

(8)

S. Blacher

C. Alie

C. Gommes

P. Lodewyckx

R. Pirard

J.-P. Pirard

Texture characterization of ultramacroporous materials using non-destructive methods

331

(8)

S. Blacher

V. Maquet

A. Leonard

G. Chapelle

M. Crine

R. Jerome

J.-P. Pirard

Formation of hierarchically ordered silicas prepared by spray drying of nanosized spheres

339

(8)

C. du Fresne von Hohenesche

V. Stathopoulos

K.K. Unger

A. Lind

M. Linden

Ultrathin porous glass membranes with controlled texture properties

347

(8)

D. Enke

F. Friedel

F. Janowski

T. Hahn

W. Gille

R. Muller

H. Kaden

Reconstruction of mesoporous silica glass Gelsil® 50

355

(8)

N. Eschricht

E. Hoinkis

F. Madler

P. Schubert-Bischoff

Pore structural characteristics of mesostructured materials prepared under different conditions

363

(8)

A.E. Candeias

M.M.L. Ribeiro-Carrott

P.J.M. Carrott

K. Schumacher

M. Grun

K.K. Unger

A grand canonical Monte Carlo simulation study of water adsorption in a Vycor-like disordered mesoporous material at 300K

371

(8)

J. Puibasset

R.J.-M. Pellenq

A review of the application of the BET equation to experimental data: the C parameter

379

(8)

F. Salvador

C. Sanchez-Jimenez

M.J. Sanchez-Montero

A. Salvador

Thermogravimetric and sorption measurement techniques/instruments

387

(8)

J.U. Keller

E. Robens

C. du Fresne von Hohenesche

Influence of method of washcoat preparation on hydrothermal stability of alumina support

395

(8)

M. Kulazynski

J. Trawczynski

J. Walendziewski

Limestone influence on PAH emissions from coal AFBC. Catalytic or/and adsorption effect?

403

(8)

A.M. Mastral

T. Garcia

M.S. Callen

J.M. Lopez

R. Murillo

M.V. Navarro

Freezing point elevation in nanospace detected directly by atomic force microscopy

411

(8)

M. Miyahara

M. Sakamoto

H. Kanda

K. Higashitani

Is it possible to obtain a coherent image of the texture of a porous material?

419

(8)

F. Noville

C. Gommes

C. Doneux

A. Brasseur

R. Pirard

J.-P. Pirard

Preparation and characterisation of Cr-Co spinels for methane oxidation in presence of sulphur compounds

427

(8)

J.R. Paredes

S. Ordonez

F.V. Diez

H. Sastre

Characterising the porous structure of Egyptian mortars using thermoporometry, mercury intrusion porometry and gas adsorption manometry

435

(8)

J. Ragai

T. Poyet

I. Beurroies

F. Rouquerol

P. Llewellyn

Monitoring fast pressure changes in gas transport and sorption analysis

443

(8)

G. Reichenauer

H.-J. Fella

J. Fricke

Effect of coke deposition on catalyst texture during catalytic cracking reaction

451

(8)

J.P. Reymond

C. Delattre

M. Forissier

Precision of porosity measurements on cementitious mortars

459

(8)

K. Rubner

Th. Fritz

F. Jacobs

Freezing in mesopores: aniline in silica glasses and MCM-41

467

(8)

M. Sliwinska-Bartkowiak

G. Dudziak

R. Radhakrishnan

K.E. Gubbins

Transport characteristics of porous solids derived from chromatographic measurements

475

(8)

O. Solcova

P. Schneider

Effects of porous solid structures on the electrical behaviour: prediction key of transport properties in sedimentary reservoir rock

483

(8)

A. Cerepi

R. Burlot

S. Galaup

J-P. Barde

C. Loisy

L. Humbert

Pore and surface characteristics of porous melamine- and phenolic-formaldehyde polymers by sorption and XPS measurements

491

(8)

A. Derylo-Marczewska

J. Goworek

Porous structure of multifunctional mineral-carbon and zeolite-carbon sorbents

499

(8)

E.B. Drag

M. Kulazynski

J. Kaczmarczyk

Waste air cleaning using activated carbon fibre cloths regenerable by direct electric heating

507

(8)

E. Schippert

C. Mohner

B. Pannwitt

H. Chmiel

Adsorption of inflammatory cytokines and endotoxin by mesoporous polymers and activated carbons

515

(6)

M.C. Murphy

S. Patel

G.J. Phillips

J.G. Davies

A. W. Lloyd

V.M. Gun'ko

S.V. Mikhalovsky

Separation of adsorption isotherms of N2 in internal and interstitial nanopores of single-walled carbon nanohorn. A comparative study with experiment and simulation

521

(8)

T. Ohba

H. Kanoh

K. Murata

M. Yudasaka

S. Iijima

K. Kaneko

Visualizing the porous structure of different carbon materials: a scanning tunneling microscopy study

529

(8)

J.I. Paredes

A. Martinez-Alonso

J.M.D. Tascon

Textural characterisation of activated carbons obtained from poly(ethylene terephthalate) by carbon dioxide activation

537

(8)

J.B. Parra

C.O. Ania

A. Arenillas

J.J. Pis

A Monte Carlo study on the structure of carbon dioxide adsorbed in microporous carbons

545

(8)

Th. A. Steriotis

G.K. Papadopoulos

A.K. Stubos

N. Kanellopoulos

Preloading of GAC by natural organic matter: effect of surface chemistry on TCE uptake

553

(8)

J.E. Kilduff

R. Srivastava

T. Karanfil

Structural studies of saccharose- and anthracene-based carbons by high-energy X-ray scattering

561

(8)

A. Szczygielska

A. Burian

S. Duber

J.C. Dore

V. Honkimaki

The dynamic adsorption behaviour of volatile organic compounds on activated carbon honeycomb monoliths

569

(8)

M. Yates

J. Blanco

M.A. Martin-Luengo

Structural properties of Cu-MCM-41 and Cu-Al-MCM-41 (Si/Al=30) catalysts

577

(8)

G. Ferraris

G. Moretti

G. Fierro

M. Lo Jacono

Comparative study of the textural properties of alumina-pillared saponites synthesised from the intercalation with various aluminium oligomers

585

(8)

L.M. Gandia

M.A. Vicente

A. Gil

Chord length distribution and pore size distribution of porous VYCOR glass

593

(8)

W. Gille

D. Enke

F. Janowski

A structural study of dehydration/rehydration of tobermorite, a model cement compound

601

(8)

A. Gmira

R.J.-M. Pellenq

I. Rannou

L. Duclaux

C. Clinard

T. Cacciaguerra

N. Lequeux

H. Van Damme

Support mesoporosity: a tool for better control of catalytic behavior of cobalt supported Fischer Tropsch catalysts

609

(8)

A. Griboval-Constant

A.Y. Khodakov

R. Bechara

V.L. Zholobenko

Textural characterization of montmorillonite pillared with aluminum/lanthanum polyoxycations

617

(8)

J.A. Morante

C. Pesquera

C. Blanco

F. Gonzalez

Influence of pH in mesoporous silica aluminas (MSA) synthesis

625

(8)

C. Rizzo

A. Carati

C. Barabino

C. Perego

G. Bellussi

The adsorption of 1-hexene and 3,3-dimethyl-1-butene on Ru-MCM 41

633

(6)

U. Singh

R.T. Williams

I.D. Salter

XPS studies of MCM 41 postmodified by a Schiff base copper complex

639

(8)

U. Singh

R.T. Williams

I.D. Salter

K.R. Hallam

Influence of synthesis conditions on surface heterogeneity of M41 type materials studied with lattice Monte Carlo

647

(8)

F.R. Siperstein

K.E. Gubbins

Porosity of chemically modified silica gels by nitrogen adsorption, position annihilation and small angle X-ray scattering

655

(8)

J. Goworek

A. Borowka

S. Pikus

J. Wawryszczuk

Preparation and characterization of porous sorbents for hot gas desulfurization

663

(8)

F. Tomas-Alonso

I. Orenes-Fernandez

J.M. Palacios-Latasa

Synthesis and characterization of MWW zeolites

671

(6)

L.M. Vtjurina

S.S. Khvoshchev

Structural analysis of oxyanion-cation complexes anchored by organic group in mesoporous silicas

677

(8)

H. Yoshitake

T. Yokoi

T. Tatsumi

Adsorption equilibrium of polar/non-polar mixtures on MCM-41: experiments and Monte Carlo simulation

685

(8)

J.-H. Yun

Y. He

M. Otero

T. Duren

N.A. Seaton

Nondestructive characterization of porous ceramics by X-ray refraction

693

(8)

K.-W. Harbich

F.E. Fensch-Kleemann

B. Rohl-Kuhn

P. Klobes

Ion-exchange properties of a novel layered titanium(IV) phosphate

701

(8)

O.A. Khainakova

A. Espina

C. Trobajo

S.A. Khainakov

J.R. Garcia

A.I. Bortun

The anomalous sorptive behaviour of ZSM-5 and Silicalite-I: observation of low pressure hysteresis in nitrogen adsorption

709

(8)

G. Kyriakou

C.R. Theocharis

Characterization of the textural properties of chemically dealuminated Y zeolites

717

(6)

R. Lopez-Fonseca

B. de Rivas

J.I. Gutierrez-Ortiz

J.R. Gonzalez-Velasco

Complementarity of microcalorimetry, manometry and gravimetry in the study of gas adsorption by microporous solids up to 50 bar

723

(8)

S. Moret

T. Poyet

D. Bigot

B. Polster

S. Crispel

J. Rouquerol

P. Llewellyn

The applicability of the Dubinin-Radushkevich equation to the very low pressure region of isotherms of various microporous solids

731

(6)

P. Lodewyckx

L. Verhoeven

Controlled porosity and surface area titania gels as novel photocatalytic washcoats

737

(8)

M. Yates

E. Garcia

The effect of geometry and axial orientation of spheroidal particles on the adsorption rate in a granular porous medium

745

(8)

F.A. Coutelieris

The effect of Peclet on the Sherwood number in high porosity granular media

753

(8)

F.A. Coutelieris

M.E. Kainourgiakis

A.K. Stubos

The application of Jantti's method for the fast calculation of equilibrium in case of multilayer adsorption

761

(8)

J.A. Poulis

C.H. Massen

E. Robens

G. Reichenauer

Characterization of controlled pore glasses by small angle X-ray scattering and evaluation of the scattering data by the indirect Fourier transformation method

769

(6)

A. Christoforides

N. Kanellopoulos

A. Mitropoulos

K.L. Stefanopoulos

K. Tarchanides

Author Index

775

(6)

Other volumes in the series

781

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Characterization of Porous Solids VI

Summary

Table of Contents

Supplemental Materials

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Characterization of Porous Solids VI

Summary

Table of Contents

Supplemental Materials

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