Inorganic Materials Synthesis and Fabrication

This up-to-date, single-source reference on the preparation of single-phase inorganic materials covers the most important methods and techniques in solid-state synthesis and materials fabrication. Presenting both fundamental background and advanced methodologies, it describes the principles of crystallography, thermodynamics, and kinetics required, addresses crystallographic and microstructural considerations, and describes various kinds of reactions. This is an excellent text for materials science and engineering, chemistry, and physics students, as well as a practical, hands-on reference for working professionals.

John N. Lalena, PhD, is an Adjunct Assistant Professor of Chemistry at the University of Maryland University College-Europe, and an Affiliate Research Assistant Professor of Chemistry at Virginia Commonwealth University in Richmond, Virginia. DAVID A. CLEARY, PhD, is Professor of Chemistry at Gonzaga University in Spokane, Washington. EVERETT E. CARPENTER, PHD, is Assistant Professor in the Department of Chemistry at Virginia Commonwealth University. NANCY F. DEAN, PHD, was formerly a research manager at Honeywell Electronic Materials and now runs her own consulting firm.

Preface	p. vii
Crystallographic and Microstructural Considerations	p. 1
Relationship Between Physical Properties and Crystallographic Symmetry	p. 4
Morphological Crystallography	p. 9
Space Lattices	p. 21
Surface and Interface Structures	p. 28
Controlled Crystal Growth and Microstructural Evolution	p. 33
Structures of Glassy and Quasicrystalline Phases	p. 44
References	p. 48
Chemical Energetics and Atomistics of Reactions and Transformations in Solids	p. 51
Equilibrium Thermodynamics	p. 53
Structural Energetics	p. 66
Grain Boundary Energy and Surface Energy Contributions	p. 73
Mass Transport and Nonequilibrium Thermodynamics	p. 83
Chemical Reaction and Phase Transformation Kinetics in Solids	p. 86
References	p. 101
Solid-Vapor Reactions	p. 105
Vapor-Phase Fundamentals	p. 105
Vapor Absorption and Adsorption	p. 109
Film Formation Basics	p. 114
Vapor-Phase Intercalation	p. 116
Physical Vapor Deposition	p. 120
Chemical Vapor Deposition	p. 125
Molecular Beam Epitaxy	p. 136
References	p. 138
Solid-Liquid Reactions	p. 141
Solid-Liquid Interface	p. 141
Crystallization, Precipitation, and Solidification	p. 142
Sol-Gel Processing	p. 167
Solvothermal and Hydrothermal Techniques	p. 171
Molten Salts and Room-Temperature Ionic Liquids	p. 173
Electrochemical Synthesis	p. 176
References	p. 179
Solid-Solid Reactions	p. 183
Solid-Solid Interface	p. 183
Ceramic Method	p. 184
Mechanical Alloying	p. 196
Combustion Synthesis	p. 199
Microwave Synthesis	p. 202
References	p. 207
Nanomaterials Synthesis	p. 211
Top-Down Methods for Fabrication of Nanocrystalline Materials	p. 213
Bottom-Up Methods for Synthesis of Nanostructured Solids	p. 216
References	p. 230
Materials Fabrication	p. 233
Influence of Structure on Materials Properties	p. 234
Deformation and Solidification Methods	p. 244
Consolidation Methods	p. 273
Summary	p. 291
References	p. 291
General Mechanical Engineering Terms	p. 295
Green Materials Synthesis and Processing	p. 297
Index	p. 299
Table of Contents provided by Ingram. All Rights Reserved.

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Inorganic Materials Synthesis and Fabrication

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