Organic Syntheses, Volume 76

The current volume continues the tradition of providing significant and interesting procedures, which should prove worthwhile to many synthetic chemists working in increasingly diverse areas. Following precedent, there is no specific or central theme to this volume.

Stephen F. Martin is an American chemist and professor of chemistry at The University of Texas at Austin. He is the M. June and J. Virgil Waggoner Regents Chair in Chemistry. Martin is a native of New Mexico, and received his B.S. degree in chemistry from the University of New Mexico in 1968, where he worked with R.N.

Resolution of 1,1'-Bl-2-Naphthol

1

(5)

Dongwei Cai

David L. Hughes

Thomas R. Verhoeven

Paul J. Reider

(R)-(+)- and (S)-(-)-2,2'-Bis-(Diphenylphosphino)-1,1'-Binaphthyl (Binap)

6

(6)

Dongwei Cai

Joseph F. Payack

Dean R. Bender

David L. Hughes

Thomas R. Verhoeven

Paul J. Reider

(4R,5R)-2,2-Dimethyl-α, α, α', α'-Tetra(Naphth-2-YL)-1,3-Dioxolane-4,5-Dimethanol from Dimethyl Tartrate and 2-Naphthyl-Magnesium Bromide

12

(11)

Albert K. Beck

Peter Gysi

Luigi La Vecchia

Dieter Seebach

(R,R)- and (S,S)-N,N'-Dimetyl-1,2-Diphenylethylene-1,2-Diamine

23

(14)

Alex Alexakis

Isabelle Aujard

Tonis Kanger

Pierre Mangeney

1S-(-)-1,3-Dithiane 1-Oxide

37

(9)

Philip C. Bulman

Jag P. Heer

Donald Bethell

Eric W. Collington

David M. Andrews

(1S,2R)-1-Aminoindan-2-OL

46

(11)

Jay F. Larrow

Ed Roberts

Thomas R. Verhoeven

Ken M. Ryan

Chris H. Senanayake

Paul J. Reider

Eric N. Jacobsen

Asymmetric Synthesis of α-Amino Acids by the Alkylation of Pseudoephedrine Glycinamide: L-Allylglycine and N-Boc-L-Allylglycine

57

(20)

Andrew G. Myers

James L. Gleason

1-Chloro-(2S,3S)-Dihydroxy-Cyclohexa-4,6-Diene

77

(9)

Tomas Hudlicky

Michele R. Stabile

David T. Gibson

Gregory M. Whited

(2S,3S)-(+)-(3-Phenylcyclo-Propyl)Methanol

86

(15)

Andre B. Charette

Helene Lebel

Synthesis of Chiral Non-Racemic Diols from (S,S)-1,2,3,4-Diepoxybutane: (2S, 3S)-Dihydroxy-1,4-Diphenylbutane

101

(9)

Michael A. Robbins

Paul N. Devine

Taeboem Oh

Preparation of Enantiomer-Ically Pure α-N,N-Dibenzylamino Aldehydes: S-2-(N,N-Dibenzyl-Amino)-3-Phenylpropanal

110

(13)

Manfred T. Reetz

Mark W. Drewes

Renate Schwickardi

Methyl (S)-2-Phthalimido-4-Oxobutanoate

123

(10)

Patrick Meffre

Philippe Durand

Francois Le Goffic

Conversion of Nitriles into Tertiary Amines: N,N-Dimethyl-Homoveratrylamine

133

(9)

Guilhem Rousselet

Patrice Capdevielle

Michel Maumy

Ethyl 5-Chloro-3-Phenylindole-2-Carboxylate

142

(9)

Alois Furstner

Achim Hupperts

Gunter Seidel

Generation and use of Lithium Pentafluoropropen-2-Olate: 4-Hydroxy-1,1,1,3,3-Pentafluoro-2-Hexanone Hydrate

151

(8)

Cheng-Ping Qian

Yu-Zhong Liu

Katsuhiko Tomooka

Takeshi Nakai

Bromofluorination of Alkenes: 1-Bromo-2-Fluoro-2-Phenyl-Propane

159

(10)

Gunter Haufe

Gerard Alvernhe

Andre Laurent

Thomas Ernet

Olav Goj

Stefan Kroger

Andreas Sattler

Mono-C-Methylation of Arylacetonitriles and Methyl Arylacetates by Dimethyl Carbonate: A General Method for the Synthesis of Pure 2-Arylpropionic Acids. 2-Phenylpropionic Acid

169

(9)

Pietro Tundo

Maurizio Selva

Andrea Bomben

(tert-Butyldimethyl Silyl)Allene

178

(11)

Andrew G. Myers

Bin Zheng

Dimethyl Squarate and its Conversion to 3-Ethenyl-4-Methoxycyclobutene-1,2-Dione and 2-Butyl-6-Ethenyl-5-Methoxy-1,4-Benzoquinone

189

(10)

Hui Liu

Craig S. Tomooka

Simon L. Xu

Benjamin R. Yerxa

Robert W. Sullivan

Yifeng Xiong

Harold W. Moore

[3 + 4] Annulation Using A [β-(Trimethylsilyl)Acryloyl] Silane and the Lithium Enolate of an α,β-Unsaturated Methyl Ketone: (1R*, 6S*, 7S*)-4-(tert-Butyldi-Methylsiloxy)-6-(Trimethyl Silyl)-Bicyclo[5.4.0] Undec-4-EN-2-One

199

(15)

Kei Takeda

Akemi Nakajima

Mika Takeda

Eiichi Yoshii

Generation of 1-Propynyllithium from (Z/E)-1-Bromo-1-Propene: 6-Phenylhex-2-YN-5-EN-4-OL

214

(7)

Dominique Toussaint

Jean Suffert

6-Chloro-1-Hexene and 8-Chloro-1-Octene

221

(7)

Pierre Mazerolles

Paul Boussaguet

Vincent Huc

Use of Cerium(III) Chloride in the Reactions of Carbonyl Compounds with Organo-Lithiums or Grignard Reagents for the Suppression of Abnormal Reactions: 1-Butyl-1,2,3,4-Tetrahydro-1-Naphthol

228

(11)

Nobuhiro Takeda

Tsuneo Imamoto

Regioselective Monoalkylation of Ketones Via their Manganese Enolates: 2-Benzyl-6-Methyl-Cyclohexanone from 2-Methyl-Cyclohexanone

239

(13)

Gerard Cahiez

Francois Chau

Bernard Blanchot

Copper-Catalyzed Conjugate Addition of Functionalized Organozinc Reagents to α,β-Unsaturated Ketones: Ethyl 5-(3-Oxocyclohexyl)Pentanoate

252

(11)

B. H. Lipshutz

M. R. Wood

R. Tirado

Isomerization of β-Alkynyl Allylic Alcohols to Furans Catalyzed by Silver Nitrate on Silica Gel: 2-Pentyl-3-Methyl-5-Heptylfuran

263

(8)

James A. Marshall

Clark A. Sehon

2-Chlorophenyl Phosphorodi-Chloridothioate

271

(4)

Vasulinga T. Ravikumar

Bruce Ross

Vitamin D2 from Ergosterol

275

(12)

Masami Okabe

5-Phenyldipyrromethane and 5,15-Diphenylporphyrin

287

(7)

Ross W. Boyle

Christian Bruckner

Jeffrey Posakony

Brian R. James

David Dolphin

9,10-Diphenylphenanthrene

294

(7)

George A. Olah

Douglas A. Klumpp

Donald N. Baek

Gebhart Neyer

Qi Wang

Unchecked Procedures

301

(4)

Cumulative Author Index for Volumes 75 and 76

305

(3)

Cumulative Subject Index for Volumes 75 and 76

308

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Organic Syntheses, Volume 76

Summary

Author Biography

Table of Contents

Supplemental Materials

FREE SHIPPING

Rent More, Save More! Use code: BBRENTAL

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Organic Syntheses, Volume 76

Summary

Author Biography

Table of Contents

Supplemental Materials

Digital License